HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Methylimidazole → HCID 178443590, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Methylimidazole | HCID 1390 | — |
| Edukt | 1-Bromooctane | HCID 8140 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 178443590 | HCID 178443590 | 90,8% |
Reaktionsschritte
1 mole of 1-methylimidazole was dissolved in 400 ml of ethanol and 1.2 moles of n-octyl bromide were added. The mixture was then heated to the boiling point for 5 hours. Thereafter, ethanol and excess n-octyl bromide were removed. The residue was purified in ether. In this manner, 250 g of 1-n-octyl-3-methyl-imidazolium bromide were obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04150967 |
| Quelldatensatz | uspto-grants-1979_04 |
| ORD ID | ord-5d047517faa743fd9d5633632be4f1d5 |
| Quellennotiz | uspto-grants-1979_04 |