HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Aminoacetaldehyde → 1-(alpha-Phenyl-o-tolyl)imidazole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Aminoacetaldehyde | HCID 363 | — |
| Edukt | Trimethyl orthoformate | HCID 9005 | — |
| Edukt | 2-Benzylaniline | HCID 119805 | — |
| Katalysator | Titanium Tetrachloride | HCID 24193 | — |
| Lösungsmittel | 1,2-Dimethoxyethane | HCID 8071 | — |
| Produkt | 1-(alpha-Phenyl-o-tolyl)imidazole | HCID 21497358 | — |
Reaktionsschritte
In the manner given in Example 1, α-phenyl-0-toluidine is reacted first with trimethyl orthoformate; the resulting product is reacted with aminoacetaldehyde, dimethyl acetal, and the resulting product of this reaction is heated with titanium tetrachloride in monoglyme to give 1-(α-phenyl-0-tolyl)imidazole.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03941802 |
| Quelldatensatz | uspto-grants-1976_03 |
| ORD ID | ord-aa4b3d1a327b410b88fda1fb97a23e75 |
| Quellennotiz | uspto-grants-1976_03 |