HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenylphosphonic Acid → Adipic Acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenylphosphonic Acid | HCID 15295 | — |
| Edukt | Hexamethylenediamine | HCID 16402 | — |
| Edukt | 6-Azaniumylhexylazanium;hexanedioate | HCID 27358 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Adipic Acid | HCID 196 | — |
Reaktionsschritte
A mixture of 100 parts of hexamethylene diammonium adipate, 0.65 part of phenylphosphonic acid, 0.48 part of hexamethylenediamine, 0.65 part of N:N'-bis(3-aminopropyl)piperazine, 0.46 part of adipic acid and 65.0 parts of water is polymerised using the conditions described in Example 1. The resulting polymer is then converted into fibres by known methods. The dye uptake of these fibres from dyebaths containing Solway Blue BN at pH's of 4.0, 7.0 and 9.0 are 8.4%, 4.7% and 1.5% respectively, compared with 4.2%, 0.6% and 0.1% for fibres prepared as described in this Example except that the phenylphosphonic acid and hexamethylenediamine were omitted from the mixture.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03944518 |
| Quelldatensatz | uspto-grants-1976_03 |
| ORD ID | ord-e71604194418479ea58f3e9332e592d0 |
| Quellennotiz | uspto-grants-1976_03 |