Diethylamine → p-[(1,5-dimethyl-hexyl)-oxy]-m-methoxy-N,N-diethyl-benzamide

HRID 267726Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 267726
[CH2:1]([NH:3][CH2:4][CH3:5])[CH3:2].CO[C:8](=[O:26])[C:9]1[CH:14]=[CH:13][C:12]([O:15][CH:16]([CH3:23])[CH2:17][CH2:18][CH2:19][CH:20]([CH3:22])[CH3:21])=[C:11]([O:24][CH3:25])[CH:10]=1>>[CH3:23][CH:16]([O:15][C:12]1[CH:13]=[CH:14][C:9]([C:8]([N:3]([CH2:4][CH3:5])[CH2:1][CH3:2])=[O:26])=[CH:10][C:11]=1[O:24][CH3:25])[CH2:17][CH2:18][CH2:19][CH:20]([CH3:21])[CH3:22]

Komponenten

3

Edukt 2

HCID 8021DiethylamineHCID 539875924-[(1,5-Dimethyl-hexyl)-oxy]-m-methoxy-benzoic acid methyl ester

Produkt 1

HCID 21487578p-[(1,5-dimethyl-hexyl)-oxy]-m-methoxy-N,N-diethyl-benzamide

Versuchsvorschrift

By the procedure described in Example 38, diethylamine is reacted with 4-[(1,5-dimethyl-hexyl)-oxy]-m-methoxy-benzoic acid methyl ester to produce 4-[(1,5-dimethyl-hexyl)-oxy]-m-methoxy-N,N-diethyl-benzamide (boiling point = 180°-182°C/0.1 mmHg).

Quellen und Nachweise

ORD-Eintrag
ord-1ad4edae407d45ffa6ddf8d3fab90d7d
Quelldatensatz
uspto-grants-1976_03
Patentnummer
US03944531

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