1,3-Cyclohexanedione → HCID 70635123, Verbindung

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	1,3-Cyclohexanedione	HCID 10434	—
Edukt	Isoquinoline-1-carbaldehyde	HCID 265306	—
Edukt	Carbamimidoyl-acetic acid ethyl ester	HCID 4599837	—
Lösungsmittel	Ethanol	HCID 702	—
Produkt	HCID 70635123	HCID 70635123	—

Reaktionsschritte

Upon heating a solution of 6.3 g of isoquinolin-1-aldehyde, 4.5 g of cyclohexane-1,3-dione and 5.2 g of amidinoacetic acid ethyl ester in 100 ml of ethanol for 2 hours, 2-amino-4-(isoquinol-1-yl)-1,4,5,6,7,8-hexahydro-5oxoquinoline-3-carboxylic acid ethyl ester of melting point 272°C (ethanol) is obtained.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US03946026
Quelldatensatz	uspto-grants-1976_03
ORD ID	ord-51d1db5cfd0a4d648c5c37f3da30872c
Quellennotiz	uspto-grants-1976_03