Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Tyramine | HCID 5610 | — |
| Edukt | Triethylammonium hydrogen carbonate | HCID 11768884 | — |
| Edukt | n-Hydroxysuccinimide biotin | HCID 86743017 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | Biotin tyramine | HCID 86746652 | — |
Reaktionsschritte
a solution of biotin-N-hydroxysuccinimide, 170 mg (0.5 mMoles), and tyramine (recrystallized from water), 68.5 mg (0.5 mMoles), in 25 ml dimethylformamide was treated with 10 ml of 1M triethylammonium bicarbonate, pH 7.5, and then heated at 50° C. for 3 hours.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05731158 |
|---|
| Quelldatensatz | uspto-grants-1998_03 |
|---|
| ORD ID | ord-989c68d91dfc4d74a9b62cfdff0165f9 |
|---|
| Quellennotiz | uspto-grants-1998_03 |
|---|
