HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol → 3-bromo-N-methylbenzene-1-sulfonamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | Methylamine | HCID 6329 | — |
| Edukt | m-Bromobenzenesulphonyl chloride | HCID 17943 | — |
| Produkt | 3-bromo-N-methylbenzene-1-sulfonamide | HCID 7213265 | 88% |
Reaktionsschritte
Prepared by general procedure III from 3-bromobenzenesulfonyl chloride (5.0 g, 20 mmol) and 2M solution of methylamine in EtOH (10.8 mL, 22 mmol) to give the title compound (4.3 g, 88%) as a white solid. MS (ISP) 250.0[(M+H)+].
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07446113B2 |
| Quelldatensatz | uspto-grants-2008_11 |
| ORD ID | ord-c1cb662eb7dc4497b92cc8a78e95fcd9 |
| Quellennotiz | uspto-grants-2008_11 |