HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(4-Bromophenyl)ethanol → HCID 16735753, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(4-Bromophenyl)ethanol | HCID 95352 | — |
| Edukt | 3-Ethynyl-8-trifluoromethyl-6-(4-trifluoromethyl-phenyl)-imidazo[1,2-a]pyridine | HCID 86608011 | — |
| Produkt | HCID 16735753 | HCID 16735753 | — |
Reaktionsschritte
The title compound was prepared from 3-ethynyl-8-trifluoromethyl-6-(4-trifluoromethyl-phenyl)-imidazo[1,2-a]pyridine (example C.18) (360 mg, 1 mmol) and commercially available 4-bromo-methylbenzyl alcohol (184 mg, 1 mmol) according to general procedure II. Obtained as an off-white solid (65 mg, 13%). MS (ISP) 475.2 [(M+H)+]; mp 157-158° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07446113B2 |
| Quelldatensatz | uspto-grants-2008_11 |
| ORD ID | ord-604c41e4def64682959c5517cb208653 |
| Quellennotiz | uspto-grants-2008_11 |