Hydrochloric Acid → Methyl 3-(sec-butylcarbamoyl)acrylate

HRID 269713

Reaktionsgleichung

[CH:1]([NH:5][C:6]([CH:8]=[CH:9][C:10]([OH:12])=[O:11])=[O:7])([CH2:3][CH3:4])[CH3:2].Cl.[CH3:14]O>>[CH:1]([NH:5][C:6]([CH:8]=[CH:9][C:10]([O:12][CH3:14])=[O:11])=[O:7])([CH2:3][CH3:4])[CH3:2]

Komponenten

Edukt 3

HCID 313Hydrochloric Acid

HCID 887Methanol

HCID 2445953-(Sec-butylcarbamoyl)acrylic acid

Produkt 1

HCID 54128810Methyl 3-(sec-butylcarbamoyl)acrylate

Versuchsvorschrift

To 3-(sec butylcarbamoyl)acrylic acid (20 g, 117 mmol) at room temperature was added 150 mL 1.2M HCl in methanol. The resulting mixture was stirred for two hours. Solvents were removed in vacuo to give the desired ester, which was used without further purification.

Aufarbeitung

customSolvents were removed in vacuo

Quellen und Nachweise

ORD-Eintrag: ord-4c7dd66728e1478c8e5011a149f328cd
Quelldatensatz: uspto-grants-2008_11
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07449242B2

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