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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 27091Erstellt: 25. Oktober 2026

1-Cyano-2-ethoxy-2-methylaminoethylene → HCID 178483853, Verbindung

https://huagongshe.com/reaction/27091

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1-Cyano-2-ethoxy-2-methylaminoethyleneHCID 73683202—
EduktHCID 178433288HCID 178433288—
LösungsmittelPyridineHCID 1049—
ProduktHCID 178483853HCID 178483853—

Reaktionsschritte

4-Methyl-5-[(2-aminoethyl)thiomethyl]imidazole (3.5 g) was added to a solution of 1-cyano-2-ethoxy-2-methylaminoethylene in pyridine (3.1 g) and the solution was stirred for 5 hours at 100°. The product was chromatographed on a column of neutral alumina with elution by chloroform/ethyl acetate (1:1) to give the title compound as a glass.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04220652
Quelldatensatzuspto-grants-1980_09
ORD IDord-10944535e2734a209418e4008f02eba6
Quellennotizuspto-grants-1980_09