HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,1-Bis(methylthio)-2-nitroethylene → 1-Nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Edukt | HCID 178510959 | HCID 178510959 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | 1-Nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene | HCID 178503821 | — |
Reaktionsschritte
A solution of 4-(4-aminobutyl)imidazole (from the dihydrobromide (3.6 g)) and 1-nitro-2,2-bis-methylthioethylene (2.0 g) in acetonitrile (50 ml) was set aside at room temperature for 3 days. The product was chromatographed on a column of silica gel to give 1-nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04220652 |
| Quelldatensatz | uspto-grants-1980_09 |
| ORD ID | ord-b946b297dc4c49f18af7ef3af86d6d42 |
| Quellennotiz | uspto-grants-1980_09 |