HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Aniline → 2-[(N-phenylcarbamoyl)methyl]prop-2-enoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Aniline | HCID 6115 | — |
| Edukt | Itaconic Anhydride | HCID 75110 | — |
| Lösungsmittel | Methyl Chloride | HCID 6327 | — |
| Produkt | 2-[(N-phenylcarbamoyl)methyl]prop-2-enoic acid | HCID 21935560 | — |
Reaktionsschritte
A solution of 2-methylenesuccinic anhydride (500 mg, 4.46 mmol) and aniline (0.4 mL, 4.46 mmol) in CH3Cl were shaken overnight. A precipitate formed, which was filtered off, washed with hexanes, and dried under vacuum to afford 2-[(N-phenylcarbamoyl)methyl]prop-2-enoic acid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07452889B2 |
| Quelldatensatz | uspto-grants-2008_11 |
| ORD ID | ord-682c33e9511d4681b3e6095fa4659f39 |
| Quellennotiz | uspto-grants-2008_11 |