HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → Acifluorfen sodium
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Acifluorfen | HCID 44073 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Acifluorfen sodium | HCID 44072 | 105,4% |
Reaktionsschritte
5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (1.7 g, 0.0047 mole) is dissolved in methanol (25 ml) and sodium hydroxide (4.7 ml of 1 N NaOH in methanol, 0.0047 mole) is added rapidly. The solvent is then removed in vacuo to give 1.9 g of product that decomposes at 217° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04220468 |
| Quelldatensatz | uspto-grants-1980_09 |
| ORD ID | ord-f721db82d1d0420393e4aedde7b519cb |
| Quellennotiz | uspto-grants-1980_09 |