Toluene → Dimethylammonium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate

HRID 27320

Reaktionsgleichung

Reaktionsgleichung von HRID 27320
[Cl:1][C:2]1[CH:20]=[C:19]([C:21]([F:24])([F:23])[F:22])[CH:18]=[CH:17][C:3]=1[O:4][C:5]1[CH:6]=[CH:7][C:8]([N+:14]([O-:16])=[O:15])=[C:9]([CH:13]=1)[C:10]([OH:12])=[O:11].[C:25]1(C)C=CC=CC=1>>[Cl:1][C:2]1[CH:20]=[C:19]([C:21]([F:22])([F:23])[F:24])[CH:18]=[CH:17][C:3]=1[O:4][C:5]1[CH:6]=[CH:7][C:8]([N+:14]([O-:16])=[O:15])=[C:9]([CH:13]=1)[C:10]([O-:12])=[O:11].[CH3:25][NH2+:14][CH3:8]

Komponenten

3

Edukt 2

HCID 1140TolueneHCID 44073Acifluorfen

Produkt 1

HCID 21280075Dimethylammonium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate

Versuchsvorschrift

5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (2.0 g) is dissolved in toluene and an excess of anhydrous dimethylamine is bubbled into the reaction mixture, the solvent removed in vacuo and the residue triturated with cold diethyl ether to give 1.1 g of product.

Aufarbeitung

  1. customan excess of anhydrous dimethylamine is bubbled into the reaction mixture
  2. customthe solvent removed in vacuo
  3. customthe residue triturated with cold diethyl ether

Quellen und Nachweise

ORD-Eintrag
ord-d9c645d4190f40a6919ff3918d90aadd
Quelldatensatz
uspto-grants-1980_09
Patentnummer
US04220468

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