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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 273309Erstellt: 26. Oktober 2026

Ethyl 2-pyridinecarboxylate → 1,5-Bis(4-ethoxy-pyridin-2-yl)pentane-1,3,5-trione

https://huagongshe.com/reaction/273309

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthyl 2-pyridinecarboxylateHCID 17307—
EduktEthyl 4-ethoxypicolinateHCID 49853411—
Produkt1,5-Bis(4-ethoxy-pyridin-2-yl)pentane-1,3,5-trioneHCID 17971932—

Reaktionsschritte

This compound is prepared in a manner analogous to that described in Example 1, Step 1, for pyridine-2-carboxylic acid ethyl ester, but instead 4-ethoxy-pyridine-2-carboxylic acid ethyl ester from Example 17 is used. The yellowish crude product is used for further syntheses without special purification steps. IR (cm−1): 1557 (vs); 1469 (w); 1436 (w); 1300 (m); 1207 (m); 1186 (m); 1035 (m); 818 (m).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07456285B2
Quelldatensatzuspto-grants-2008_11
ORD IDord-fcfd0baf446f430c93ca8c16ecd91c11
Quellennotizuspto-grants-2008_11