Tridecanal → 2,3-Dihydro-1,3-dimethyl-2-dodecylperimidine

HRID 274156

Reaktionsgleichung

Reaktionsgleichung von HRID 274156
[CH3:1][NH:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][C:11]=2[NH:13][CH3:14])[CH:6]=[CH:5][CH:4]=1.[CH:15](=O)[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27]>>[CH3:14][N:13]1[C:11]2=[C:12]3[C:7](=[CH:8][CH:9]=[CH:10]2)[CH:6]=[CH:5][CH:4]=[C:3]3[N:2]([CH3:1])[CH:15]1[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27]

Komponenten

3

Edukt 2

HCID 25311TridecanalHCID 140748N,N'-Dimethyl-1,8-naphthalenediamine

Produkt 1

HCID 154041002,3-Dihydro-1,3-dimethyl-2-dodecylperimidine

Versuchsvorschrift

N,N'-dimethyl-1,8-naphthalene diamine was first prepared and condensed with tridecanal to give 2,3-dihydro-1,3-dimethyl-2-dodecylperimidine. The 2,3-dihydroperimidine was coupled with the his diazonium salt prepared in Example 12 to give the above blue dye.

Quellen und Nachweise

ORD-Eintrag
ord-471579593d4b4bf1bbe61829666584f0
Quelldatensatz
uspto-grants-1995_02
Patentnummer
US05389285

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