HCID 15239992, Verbindung → methyl 6-(N,N-dimethylamino)-3-hydroxypicolinate
Reaktionsgleichung
C([O:8][C:9]1[C:10]([C:18]([O:20][CH3:21])=[O:19])=[N:11][C:12]([N:15]([CH3:17])[CH3:16])=[CH:13][CH:14]=1)C1C=CC=CC=1>[C].[Pd].C(OCC)(=O)C>[CH3:17][N:15]([C:12]1[N:11]=[C:10]([C:18]([O:20][CH3:21])=[O:19])[C:9]([OH:8])=[CH:14][CH:13]=1)[CH3:16]Komponenten
4
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 2
Versuchsvorschrift
2.3 g (8 mmol) of methyl 3-benzyloxy-6-(N,N-dimethylamino)picolinate and 0.3 g of 10% palladium carbon were added to 100 ml of ethyl acetate, and was hydrogenated under normal pressure, after the reaction, the reaction product was filtrated and concentrated to obtain a crystal.
Aufarbeitung
- customafter the reaction
- filtrationthe reaction product was filtrated
- concentrationconcentrated
- customto obtain a crystal
Quellen und Nachweise
- ORD-Eintrag
- ord-d4b79056edcf4a36b03943e9afab1acc
- Quelldatensatz
- uspto-grants-1995_02
- Patentnummer
- US05391537
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