Methylamine → HCID 178484966, Verbindung

Reaktionsgleichung

OC[C:3]1[N:8]=[CH:7]C=[CH:5][N:4]=1.SCCC[NH2:13].[NH2:14][CH2:15][CH2:16][CH2:17][S:18][CH2:19][C:20]1[N:25]=[CH:24][CH:23]=[CH:22][N:21]=1.CN>>[C:5]([NH:4][C:3]([NH:8][CH3:7])=[N:14][CH2:15][CH2:16][CH2:17][S:18][CH2:19][C:20]1[N:21]=[CH:22][CH:23]=[CH:24][N:25]=1)#[N:13]

Komponenten

Edukt 4

HCID 6329Methylamine

HCID 974361-Propanethiol, 3-amino-

HCID 27630242-Pyrimidinemethanol

HCID 205675642-[(3-Aminopropyl)thiomethyl]pyrimidine

Produkt 1

HCID 178484966HCID 178484966, Verbindung

Versuchsvorschrift

Also, reacting 2-hydroxymethylpyrimidine with 3-mercaptopropylamine by the procedure of Example 1 and then reacting the resulting 2-[(3-aminopropyl)thiomethyl]-pyrimidine with dimethyl-N-cyanoimidodithiocarbonate and methylamine by the procedure of Example 3(d) gives N-cyano-N'-methyl-N"-[3-(2-pyrimidylmethylthio)propyl]guanidine.