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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 275057Erstellt: 26. Oktober 2026

Triethyl Citrate → 1,2,3-Triethyl 1,2,3-propanetricarboxylate

https://huagongshe.com/reaction/275057

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTriethyl CitrateHCID 6506—
EduktHCID 178418361HCID 178418361—
LösungsmittelEthanolHCID 702—
Produkt1,2,3-Triethyl 1,2,3-propanetricarboxylateHCID 22105554%

Reaktionsschritte

400 ml of triethyl citrate were hydrogenated at 175° C. and 10 bar together with 1100 ml of ethanol and 60 g of catalyst B (4-mm pellets) until the take-up of hydrogen had ceased. The reaction product was freed from ethanol and distilled under reduced pressure, giving 231.8 g (54%) of triethyl 1,2,3-propanetricarboxylate.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05391771
Quelldatensatzuspto-grants-1995_02
ORD IDord-b23b886bceb04fb4aabb1173fd5720d5
Quellennotizuspto-grants-1995_02