HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethyl Citrate → 1,2,3-Triethyl 1,2,3-propanetricarboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethyl Citrate | HCID 6506 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 1,2,3-Triethyl 1,2,3-propanetricarboxylate | HCID 221055 | 54% |
Reaktionsschritte
400 ml of triethyl citrate were hydrogenated at 175° C. and 10 bar together with 1100 ml of ethanol and 60 g of catalyst B (4-mm pellets) until the take-up of hydrogen had ceased. The reaction product was freed from ethanol and distilled under reduced pressure, giving 231.8 g (54%) of triethyl 1,2,3-propanetricarboxylate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05391771 |
| Quelldatensatz | uspto-grants-1995_02 |
| ORD ID | ord-b23b886bceb04fb4aabb1173fd5720d5 |
| Quellennotiz | uspto-grants-1995_02 |