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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 275061Erstellt: 26. Oktober 2026

Triethyl Citrate → 1,2,3-Triethyl 1,2,3-propanetricarboxylate

https://huagongshe.com/reaction/275061

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTriethyl CitrateHCID 6506—
EduktTetrahydrofuranHCID 8028—
EduktHCID 178418361HCID 178418361—
LösungsmittelEthanolHCID 702—
Produkt1,2,3-Triethyl 1,2,3-propanetricarboxylateHCID 22105545%

Reaktionsschritte

400 ml of triethyl citrate were hydrogenated at 175° C. and 10 bar together with 1100 ml of tetrahydrofuran and 60 g of catalyst G (4-mm tablets) until the take-up of hydrogen had ceased. The reaction product was freed from ethanol and distilled under reduced pressure, giving 193 g (45%) of triethyl propane-1,2,3-tricarboxylate.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05391771
Quelldatensatzuspto-grants-1995_02
ORD IDord-fdfd6c8e013d482092b9552ae9442a80
Quellennotizuspto-grants-1995_02