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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 275251Erstellt: 26. Oktober 2026

2-Methylbenzothiazole → 2-Methyl-3-(5-carboxypentyl) benzothiazolium bromide

https://huagongshe.com/reaction/275251

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-MethylbenzothiazoleHCID 8446—
Edukt6-Bromohexanoic acidHCID 20210—
Produkt2-Methyl-3-(5-carboxypentyl) benzothiazolium bromideHCID 22930888212,9%

Reaktionsbedingungen

Temperatur120 °C

Reaktionsschritte

2-methyl benzothiazole (19.5g, 0.1M) and 6-bromohexanoic acid (15.3g, 0.1M) were mixed and heated at 120° C. for 4 hours under continuous agitation. The resulting solid was broken up, ground with ether and then filtered. The filtrate was washed with more ether (250ml) to yield an off-white powder (57.5g).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05393654
Quelldatensatzuspto-grants-1995_02
ORD IDord-e9b9ffc8121942548db3ebc77f1545c8
Quellennotizuspto-grants-1995_02