Ethylenediamine → N-(3-isothiazolylmethyl)ethylenediamine

HRID 27558Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 27558
[CH2:1]([NH2:4])[CH2:2][NH2:3].Br[CH2:6][C:7]1[CH:11]=[CH:10][S:9][N:8]=1>>[S:9]1[CH:10]=[CH:11][C:7]([CH2:6][NH:3][CH2:2][CH2:1][NH2:4])=[N:8]1

Komponenten

3

Edukt 2

HCID 3301EthylenediamineHCID 130375983-(bromomethyl)Isothiazole

Produkt 1

HCID 20557777N-(3-isothiazolylmethyl)ethylenediamine

Versuchsvorschrift

By the procedure of Example 34, ethylenediamine is reacted with 3-bromomethylisothiazole to give N-(3-isothiazolylmethyl)ethylenediamine. This intermediate is heated under reflux with S-methylisothiouronium sulphate in water for 3 hours by the procedure of Example 1 to give the title compound.

Quellen und Nachweise

ORD-Eintrag
ord-fcd79cf2735a42a88f42510c755d112b
Quelldatensatz
uspto-grants-1980_09
Patentnummer
US04221802

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