HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl 3-chloro-4-hydroxyphenylacetate → (3-Chloro-4-((4-isobutylbenzyl)oxy)phenyl)acetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl 3-chloro-4-hydroxyphenylacetate | HCID 92625 | — |
| Edukt | 1-(Chloromethyl)-4-(2-methylpropyl)benzene | HCID 181289 | — |
| Lösungsmittel | Methanol--water (1/1) | HCID 22242641 | — |
| Produkt | (3-Chloro-4-((4-isobutylbenzyl)oxy)phenyl)acetic acid | HCID 3248707 | — |
Reaktionsschritte
3-chloro-4-(4'-isobutylbenzyloxy) phenylacetic acid was prepared in accordance with the procedure designated (f) above by reacting 4-isobutylbenzyl chloride and methyl 3-chloro-4-hydroxyphenylacetate. The resultant product evidenced a melting point of 97°-99° C. (methanol-water 4:1), the yield being 61%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04221919 |
| Quelldatensatz | uspto-grants-1980_09 |
| ORD ID | ord-471735454f1e4fe78614209bad414c09 |
| Quellennotiz | uspto-grants-1980_09 |