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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 276360Erstellt: 25. Oktober 2026

1,2-Dichloro-4-isothiocyanatobenzene → 2-(3,4-Dichlorophenylimino)-3-(cyclobutylmethyl)-1,3-thiazolidine

https://huagongshe.com/reaction/276360

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1,2-Dichloro-4-isothiocyanatobenzeneHCID 23065—
EduktN-cyclobutylmethyl-N-(2-chloroethyl)ammonium chlorideHCID 18316353—
Produkt2-(3,4-Dichlorophenylimino)-3-(cyclobutylmethyl)-1,3-thiazolidineHCID 18316044—

Reaktionsschritte

2-Hydroxyethylamine was reacted with cyclobutylmethyl bromide according to Method B2a to give N-cyclobutylmethyl-N-(2-hydroxyethyl)amine. The alcohol was reacted with SOCl2 according to Method B7c to give N-cyclobutylmethyl-N-(2-chloroethyl)ammonium chloride. The chloroethylamine was reacted with 3,4-dichlorophenyl isothiocyanate to give 2-(3,4-dichlorophenylimino)-3-(cyclobutylmethyl)-1,3-thiazolidine.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06353006B1
Quelldatensatzuspto-grants-2002_03
ORD IDord-cfd7ff92352e4f07a34b7f9d8114bc0c
Quellennotizuspto-grants-2002_03