2,3-Dimethylphenylisothiocyanate → HCID 18315967, Verbindung

HRID 276363

Reaktionsgleichung

Reaktionsgleichung von HRID 276363
[Cl-].[CH:2]1([CH2:6][NH2+:7][CH2:8][CH2:9]Cl)[CH2:5][CH2:4][CH2:3]1.[CH3:11][C:12]1[C:17]([CH3:18])=[CH:16][CH:15]=[CH:14][C:13]=1[N:19]=[C:20]=[S:21]>>[CH3:11][C:12]1[C:17]([CH3:18])=[CH:16][CH:15]=[CH:14][C:13]=1[N:19]=[C:20]1[N:7]([CH2:6][CH:2]2[CH2:5][CH2:4][CH2:3]2)[CH2:8][CH2:9][S:21]1

Komponenten

3

Edukt 2

HCID 1370682,3-DimethylphenylisothiocyanateHCID 18316353N-cyclobutylmethyl-N-(2-chloroethyl)ammonium chloride

Produkt 1

HCID 18315967HCID 18315967, Verbindung

Versuchsvorschrift

2-Hydroxyethylamine was reacted with cyclobutylmethyl bromide according to Method B2a to give N-cyclobutylmethyl-N-(2-hydroxyethyl)amine. The alcohol was reacted with SOCl2 according to Method B7c to give N-cyclobutylmethyl-N-(2-chloroethyl)ammonium chloride. The chloroethylamine was reacted with 2,3-dimethylphenyl isothiocyanate to give 2-(2,3-dimethylphenylimino)-3-(cyclobutylmethyl)-1,3-thiazolidine.

Quellen und Nachweise

ORD-Eintrag
ord-18181f417cd740a6af8f6affedba33ce
Quelldatensatz
uspto-grants-2002_03
Patentnummer
US06353006B1

Verknüpfte Notizen

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