HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzylethanolamine → N-(2-Chloroethyl)benzylamine hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzylethanolamine | HCID 4348 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Produkt | N-(2-Chloroethyl)benzylamine hydrochloride | HCID 22712 | — |
Reaktionsschritte
2-Hydroxyethylamine was reacted with benzyl bromide according to Method B2a to give N-benzyl-N-(2-hydroxyethyl)amine. The alcohol was reacted with SOCl2 according to Method B7c to give N-benzyl-N-(2-chloroethyl)ammonium chloride. The chloroethylamine was reacted with 3-chloro-2-methylphenyl isothiocyanate to give 2-(3-chloro-2-methylphenylimino)-3-benzyl-1,3-thiazolidine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06353006B1 |
| Quelldatensatz | uspto-grants-2002_03 |
| ORD ID | ord-3f1bead79d844ede9672e83212651828 |
| Quellennotiz | uspto-grants-2002_03 |