Ethanolamine → N-cycloheptylmethyl-N-(2-hydroxyethyl)amine

HRID 276426Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 276426
[OH:1][CH2:2][CH2:3][NH2:4].[CH:5]1([CH2:12]Br)[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6]1>>[CH:5]1([CH2:12][NH:4][CH2:3][CH2:2][OH:1])[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6]1

Komponenten

3

Edukt 2

HCID 700EthanolamineHCID 23000753(Bromomethyl)cycloheptane

Produkt 1

HCID 18316190N-cycloheptylmethyl-N-(2-hydroxyethyl)amine

Versuchsvorschrift

2-Hydroxyethylamine was reacted with cycloheptylmethyl bromide according to Method B2a to give N-cycloheptylmethyl-N-(2-hydroxyethyl)amine. The alcohol was reacted with SOCl2 according to Method B7c to give N-cycloheptylmelthyl-N-(2-chloroethyl)ammonium chloride. The chloroethylamine was reacted with 4-cyanophenyl isothiocyanate to give 2-(4-cyanophenylimino)-3-(cycloheptylmethyl)-1,3-thiazolidine.

Quellen und Nachweise

ORD-Eintrag
ord-f7b051e3e586404ca8770b95779f3486
Quelldatensatz
uspto-grants-2002_03
Patentnummer
US06353006B1

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