HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-ethoxymethylene-2-(1)-naphthyl-5(4H)-oxazolone → 4-{4-[(benzylidene-amino)-methyl]-piperidin-1-ylmethylene}-2-naphthalen-1-yl-4H-oxazol-5-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-ethoxymethylene-2-(1)-naphthyl-5(4H)-oxazolone | HCID 356930 | — |
| Edukt | N-Benzylidene(piperidin-4-yl)methanamine | HCID 11820173 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 4-{4-[(benzylidene-amino)-methyl]-piperidin-1-ylmethylene}-2-naphthalen-1-yl-4H-oxazol-5-one | HCID 54057694 | — |
Reaktionsschritte
To a solution of 4-ethoxymethylene-2-naphthalen-1-yl-4H-oxazol-5-one (11.40 g, 43 mmol) in tetrahydrofuran, benzylidene-piperidin-4-ylmethyl-amine (8.60 g, 43 mmol) was added, and the mixture was stirred at room temperature for 24 h. The reaction mixture was concentrated under reduced pressure to yield 4-{4-[(benzylidene-amino)-methyl]-piperidin-1-ylmethylene}-2-naphthalen-1-yl-4H-oxazol-5-one.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06355641B1 |
| Quelldatensatz | uspto-grants-2002_03 |
| ORD ID | ord-0ea03cc5fb7f4f1cb7f181c2ebd1448a |
| Quellennotiz | uspto-grants-2002_03 |