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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 276787Erstellt: 25. Oktober 2026

4-ethoxymethylene-2-(1)-naphthyl-5(4H)-oxazolone → 4-{4-[(benzylidene-amino)-methyl]-piperidin-1-ylmethylene}-2-naphthalen-1-yl-4H-oxazol-5-one

https://huagongshe.com/reaction/276787

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4-ethoxymethylene-2-(1)-naphthyl-5(4H)-oxazoloneHCID 356930—
EduktN-Benzylidene(piperidin-4-yl)methanamineHCID 11820173—
LösungsmittelTetrahydrofuranHCID 8028—
Produkt4-{4-[(benzylidene-amino)-methyl]-piperidin-1-ylmethylene}-2-naphthalen-1-yl-4H-oxazol-5-oneHCID 54057694—

Reaktionsschritte

To a solution of 4-ethoxymethylene-2-naphthalen-1-yl-4H-oxazol-5-one (11.40 g, 43 mmol) in tetrahydrofuran, benzylidene-piperidin-4-ylmethyl-amine (8.60 g, 43 mmol) was added, and the mixture was stirred at room temperature for 24 h. The reaction mixture was concentrated under reduced pressure to yield 4-{4-[(benzylidene-amino)-methyl]-piperidin-1-ylmethylene}-2-naphthalen-1-yl-4H-oxazol-5-one.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06355641B1
Quelldatensatzuspto-grants-2002_03
ORD IDord-0ea03cc5fb7f4f1cb7f181c2ebd1448a
Quellennotizuspto-grants-2002_03