3-(3-Pyridinyl)-2-propenenitrile → 2-Phenyl-7-pyridin-3-yl-[1,2,4]triazolo[1,5-a]pyridin-5-ylamine
Reaktionsgleichung
C1(S([CH2:10][C:11]2[N:15]=[C:14]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)[NH:13][N:12]=2)(=O)=O)C=CC=CC=1.[N:22]1[CH:27]=[CH:26][CH:25]=[C:24]([CH:28]=[CH:29][C:30]#[N:31])[CH:23]=1>>[C:16]1([C:14]2[N:15]=[C:11]3[CH:10]=[C:28]([C:24]4[CH:23]=[N:22][CH:27]=[CH:26][CH:25]=4)[CH:29]=[C:30]([NH2:31])[N:12]3[N:13]=2)[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=1Komponenten
3
Versuchsvorschrift
The title compound, mp. 201-203° C., MS m/e (%): 288 (M+H+, 100), was prepared in accordance with the general method of example 22 from 3-benzenesulfonylmethyl-5-phenyl-1H-[1,2,4]triazole and 3-pyridin-3-yl-acrylonitrile.
Quellen und Nachweise
- ORD-Eintrag
- ord-6ca0b8e87c9b4bb1874803e11d19e5ba
- Quelldatensatz
- uspto-grants-2002_03