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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 277641Erstellt: 26. Oktober 2026

Benzoyl chloride → (3-Tert-butyl-4-hydroxyphenyl) benzoate

https://huagongshe.com/reaction/277641

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzoyl chlorideHCID 7412—
EduktTert-ButylhydroquinoneHCID 16043—
LösungsmittelPyridineHCID 1049—
Produkt(3-Tert-butyl-4-hydroxyphenyl) benzoateHCID 836814—

Reaktionsschritte

Using 6.65 g of 2-tert-butyl-1,4-dihydroxybenzene, 4.6 ml of benzoyl chloride and 200 ml of pyridine, reaction and workup carried out as in Reference Example gave 9.35 g of 4-benzoyloxy-2-tert-butylphenol as white crystals, m.p. 120-121° C. Using. 9.35 g of the white crystals, 1,47 g of sodium hydride, 6.27 g of benzyl bromide and 40 ml of DMF, reaction and workup carried out as in Example 12 gave 6.07 g of yellow oil.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06358515B2
Quelldatensatzuspto-grants-2002_03
ORD IDord-195d0e7013504a89bdc9616bbea8d83a
Quellennotizuspto-grants-2002_03