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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 277646Erstellt: 25. Oktober 2026

Triethylamine → HCID 22625376, Verbindung

https://huagongshe.com/reaction/277646

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTriethylamineHCID 8471—
Edukt((p-(Benzyloxy)phenoxy)methyl)oxiraneHCID 119882—
Edukt1-(2,5-Dimethoxyphenyl)piperazine dihydrochlorideHCID 13599003—
Lösungsmittel1,4-DioxaneHCID 31275—
ProduktHCID 22625376HCID 2262537633,9%

Reaktionsschritte

2.56 g of 1-(4-benzyloxyphenoxy)-2,3-epoxypropane was dissolved in 100 ml of dioxane, and to this were added 2.95 g of 1-(2,5-dimethoxyphenyl)piperazine dihydrochloride and 3.5 ml of triethylamine and reaction and workup were carried out as in Example 1-A. The residue obtained was purified by column chromatography (silica gel, elution with ethyl acetate:hexane=1:1) to give 1.62 g of brown oil.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06358515B2
Quelldatensatzuspto-grants-2002_03
ORD IDord-74ab6cf6ea5342a989d4f284f57cbbbb
Quellennotizuspto-grants-2002_03