HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Toluenesulfonyl chloride → 6-Phenylhexyl tosylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | 6-Phenyl-1-hexanol | HCID 520110 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 6-Phenylhexyl tosylate | HCID 10688038 | 100% |
Reaktionsschritte
A solution of 6-phenyl-1-hexanol (2.9 g, 16.27 mmoles), CH2Cl2 (30 ml), triethylamine (4.76 ml, 34.16 mmoles) and p-toluensulphonyl chloride (3.26 g, 17.08 mmoles) was kept under stirring at room temperature for 1 night, washed with water, 5% HCl and NaHCO3 and evaporated to give 5.4 g of the title compound (yield: 100%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06358973B1 |
| Quelldatensatz | uspto-grants-2002_03 |
| ORD ID | ord-414b3bc4d1df41b483bbbd1d480741fb |
| Quellennotiz | uspto-grants-2002_03 |