1,3-Di(3-methyl-3-hydroxy-1-butynyl)benzene → Mesitylene

HRID 27801Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 27801
[CH3:1]C(O)(C#CC1C=CC=C(Br)C=1)C.CC(O)(C)C#[C:17][C:18]1[CH:23]=[CH:22][CH:21]=[C:20]([C:24]#CC(O)(C)C)[CH:19]=1>>[C:18]1([CH3:17])[CH:19]=[C:20]([CH3:24])[CH:21]=[C:22]([CH3:1])[CH:23]=1

Komponenten

3

Edukt 2

HCID 50980371,3-Di(3-methyl-3-hydroxy-1-butynyl)benzeneHCID 23006378HCID 23006378, Verbindung

Produkt 1

HCID 7947Mesitylene

Versuchsvorschrift

Referring to Table 1 above, the Conversion ("Conv.") was a weight percent conversion and was calculated by: ##EQU1## Selectivity ("Selec.") in Table 1 means, as appropriate: ##EQU2## The Yield means, as appropriate, the yield of 2-methyl-4-(3-bromophenyl)-3-butyn-2-ol: ##STR15## or 1,3-di(3-methyl-3-hydroxy-1-butynyl)benzene: ##STR16## and was calculated as the product of Conversion times Selectivity. Selectivities and yields were calculated only on isolated crude products by gas chromatography with an appropriate internal standard (mesitylene).

Aufarbeitung

  1. customSelectivities and yields

Quellen und Nachweise

ORD-Eintrag
ord-ec37ad1be5cf4fbbb5e7f1bbdb274c51
Quelldatensatz
uspto-grants-1980_09
Patentnummer
US04223172

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