HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,3,5-Trimethylphenol → 2,3,5-Trimethyl-phenyl ethyl ether
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,3,5-Trimethylphenol | HCID 12769 | — |
| Edukt | 4-Ethoxy-2,3,6-trimethyl-benzyl-triphenylphosphonium chloride | HCID 86735901 | — |
| Produkt | 2,3,5-Trimethyl-phenyl ethyl ether | HCID 20210010 | — |
Reaktionsschritte
The 4-ethoxy-2,3,6-trimethyl-benzyl-triphenylphosphonium chloride employed as the starting material is prepared by the procedure described in Example 18 by alkylation of 2,3,5-trimethylphenol to give 2,3,5-trimethyl-phenyl ethyl ether (melting point 93°-95° C.), by haloformylation of the ether obtained to give 4-ethoxy-2,3,6-trimethyl-benzyl chloride (melting point 63°-64° C.) and by reaction of the latter compound with triphenylphosphine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04224244 |
| Quelldatensatz | uspto-grants-1980_09 |
| ORD ID | ord-3dae91d07f994f6abbe906618bf1815a |
| Quellennotiz | uspto-grants-1980_09 |