Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Diisopropylamine | HCID 7912 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 4-Bromobenzyl bromide | HCID 68527 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | 4-Bromo-N,N-diisopropylbenzylamine | HCID 598770 | — |
Reaktionsschritte
A mixture of 4-bromobenzylbromide (5.0 g), N,N-diisopropylamine (7.85 ml) and potassium carbonate (2.76 g) in dimethylformamide (50 ml) was stirred at 80° C. for 2 hours. To the mixture was added water, and the mixture was extracted with ether. The extract was washed with water, dried (MgSO4) and concentrated to give the title compound (5.0 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US06359134B1 |
|---|
| Quelldatensatz | uspto-grants-2002_03 |
|---|
| ORD ID | ord-0947629a38f245a280dfe00ef647a3cd |
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| Quellennotiz | uspto-grants-2002_03 |
|---|
