HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl carbazate → N-(methoxycarbonyl)-N'-(2-benzylcyclohexylidene)-hydrazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl carbazate | HCID 80519 | — |
| Edukt | 2-Benzylcyclohexan-1-one | HCID 98945 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | N-(methoxycarbonyl)-N'-(2-benzylcyclohexylidene)-hydrazine | HCID 57106415 | 96,9% |
Reaktionsschritte
18.83 g (0.1 mole) of 2-benzylcyclohexan-1-one and 9.0 g (0.1 mole) of N-methoxycarbonyl hydrazine are dissolved in 100 cm3 of anhydrous ethanol, and the solution is boiled for 2 hours. Then it is cooled, and the separated crystals are filtered off. 18.2 g (96.9%) of the named compound are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04587261 |
| Quelldatensatz | uspto-grants-1986_05 |
| ORD ID | ord-22f0f84b0feb478f8e647024c2ae3d75 |
| Quellennotiz | uspto-grants-1986_05 |