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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 279907Erstellt: 23. Oktober 2026

Triclosan → 5-Chloro-2-(2,4-dichlorophenoxy)phenyl 2-octanoyloxy-1-(octanoyloxymethyl)ethyl adipate

https://huagongshe.com/de/reaction/279907

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTriclosanHCID 5564—
EduktAdipoyl chlorideHCID 61034—
Edukt1,3-Dioctanoyl glycerolHCID 150911—
Produkt5-Chloro-2-(2,4-dichlorophenoxy)phenyl 2-octanoyloxy-1-(octanoyloxymethyl)ethyl adipateHCID 5379861733%

Reaktionsschritte

Using a similar procedure to that described in Example 6, but using 5-chloro-2-(2,4-dichlorophenoxy)phenol, adipoyl dichloride and 2-hydroxy-3-octanoyloxypropyl octanoate as starting materials, there was obtained 5-chloro-2-(2,4-dichlorophenoxy)phenyl 2-octanoyloxy-1-(octanoyloxymethyl)ethyl adipate as an oil in 33% yield; NMR (CDCL3): 0.85 (6H, br.s, CH3), 1.25+1.65 (24H, br.s, CH2), 2.3 (8H, m, COCH2), 4.2 (4H, m, OCH2), 5.25 (1H, m, CH), 6.6-7.5 (6H, complex, aromatic H)ppm.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04587262
Quelldatensatzuspto-grants-1986_05
ORD IDord-962d4d809c1646448aff1daaf2ff3aae
Quellennotizuspto-grants-1986_05