Ammonia → D-Ribopyranosyl amine

HRID 279925

Reaktionsgleichung

Reaktionsgleichung von HRID 279925
O=[CH:2][C@@H:3]([C@@H:5]([C@@H:7]([CH2:9][OH:10])[OH:8])[OH:6])[OH:4].[Cl-].[NH4+:12].N>CO>[CH:9]1([NH2:12])[O:10][CH2:2][C@@H:3]([OH:4])[C@@H:5]([OH:6])[C@H:7]1[OH:8]

Komponenten

5

Edukt 3

HCID 222AmmoniaHCID 25517Ammonium ChlorideHCID 5311110Aldehydo-D-ribose

Produkt 1

HCID 54279899D-Ribopyranosyl amineAusbeute 932,5 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

To 100 ml of methanol was added 20 g of D-ribose and 0.5 g of ammonium chloride. This mixture was treated with anhydrous ammonia at 0° C. until a solution was obtained. This solution was stored at 0° C. for 13 days, then the solid was collected, giving 13 g of D-ribopyranosylamine.

Aufarbeitung

  1. customwas obtained
  2. customthe solid was collected

Quellen und Nachweise

ORD-Eintrag
ord-6c82f99df2f64048a4c2ef165cd553e6
Quelldatensatz
uspto-grants-1986_05
Patentnummer
US04587331

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