4-Ethylbenzoic Acid → 4-Ethylbenzoyl chloride
Reaktionsgleichung
[CH2:1]([C:3]1[CH:11]=[CH:10][C:6]([C:7](O)=[O:8])=[CH:5][CH:4]=1)[CH3:2].S(Cl)([Cl:14])=O>>[CH2:1]([C:3]1[CH:11]=[CH:10][C:6]([C:7]([Cl:14])=[O:8])=[CH:5][CH:4]=1)[CH3:2]Komponenten
3
Versuchsvorschrift
200 g (1.33 millimoles) of 4-ethylbenzoic acid are added rapidly to 500 ml of thionyl chloride with stirring. The mixture is heated at the reflux temperature for 4 hours. After evaporation of the SOCl2 and distillation, 4-ethylbenzoyl chloride is obtained.
Aufarbeitung
- temperatureThe mixture is heated at the reflux temperature for 4 hours
- customAfter evaporation of the SOCl2 and distillation
Quellen und Nachweise
- ORD-Eintrag
- ord-26a1f02e2dba46d39f0ba1c267c7aba8
- Quelldatensatz
- uspto-grants-1986_05
- Patentnummer
- US04588748
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