HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → HCID 178418442, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Benzenediazonium chloride | HCID 60992 | — |
| Edukt | 3-Oxo-n,n-dipropylbutanamide | HCID 249207 | — |
| Edukt | HCID 178418247 | HCID 178418247 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 178418442 | HCID 178418442 | 14,5% |
Reaktionsschritte
18.5 g (0.1 mol) of N,N-dipropyl-3-oxobutyramide, 12 g (0.146 mol) of CH3COONa, 20 ml of water, 75 ml of ethanol and a solution of 0.1 mol of phenyldiazonium chloride were treated as described in preparation 2. The precipitated solid was filtered and dried in vacuo yielding 4.2 g of the title compound. M.p.=79°-80° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05731322 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-549c90cb2eaf4302a24586469500c664 |
| Quellennotiz | uspto-grants-1998_03 |