HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetoacetanilide → HCID 178418293, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetoacetanilide | HCID 7592 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Benzenediazonium chloride | HCID 60992 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | HCID 178418293 | HCID 178418293 | 47,6% |
Reaktionsschritte
4.5 g (25.4 mmol) of acetoacetanilide, a solution of 3.46 g (89 mmol) of NaOH in 45 ml of water and 95 mmol of phenyldiazonium chloride were treated as described in preparation 8. The residue was crystallised from EtOH, yielding 3.4 g of the title compound. M.p.=96°-97° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05731322 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-f388a24479e44c98bc290884466e1ad3 |
| Quellennotiz | uspto-grants-1998_03 |