HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Phenylisobutyric acid → 2-Methyl-2-phenylpropanoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Phenylisobutyric acid | HCID 13222 | — |
| Edukt | Oxalyl chloride | HCID 65578 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 2-Methyl-2-phenylpropanoyl chloride | HCID 12369086 | — |
Reaktionsschritte
A solution of 2-Methyl-2-phenylpropionic acid (10 mmol, 1.0 eq.) and oxalyl chloride (40 mmol, 4.0 eq.) in dichloromethane (30 mL) was stirred at room temperature for 18 h. The mixture was concentrated in vacuo to afford the title compound as a yellow oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07420055B2 |
| Quelldatensatz | uspto-grants-2008_09 |
| ORD ID | ord-b388f55835f0450eb8040b6671d8a7a3 |
| Quellennotiz | uspto-grants-2008_09 |