Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Tributylvinyltin | HCID 81998 | — |
| Edukt | Ethyl 3-(bromophenyl)acetate | HCID 11470552 | — |
| Katalysator | HCID 178418397 | HCID 178418397 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | Ethyl 2-(3-vinylphenyl)acetate | HCID 11687033 | — |
Reaktionsschritte
A mixture of 1.0 mmol of ethyl 3-bromophenylacetate, 1.5 mmol of vinyltributyltin, and 0.1 mmol of Pd(PPh3)4 in 4 mL DMF was stirred and heated at 90° C. for 1-16 h. Chromatography provided ethyl 3-vinylphenylacetate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05731432 |
|---|
| Quelldatensatz | uspto-grants-1998_03 |
|---|
| ORD ID | ord-22f4a8336221412198601584d84cd4b1 |
|---|
| Quellennotiz | uspto-grants-1998_03 |
|---|
