Triethylamine → HCID 58794783, Verbindung

HRID 29730

Reaktionsgleichung

Reaktionsgleichung von HRID 29730
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.C1(C)[C:12]([NH2:19])=[C:13]([CH3:18])[C:14](N)=[CH:15][CH:16]=1.C([N:23]([CH2:26][CH3:27])[CH2:24][CH3:25])C>CS(C)=O>[N+:8]([C:5]1[CH:6]=[CH:7][C:2]([NH:19][CH2:12][C:13]2[CH:14]=[CH:15][CH:16]=[C:27]([CH2:26][NH:23][C:24]3[CH:25]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=3)[CH:18]=2)=[CH:3][CH:4]=1)([O-:10])=[O:9]

Komponenten

5

Edukt 3

HCID 8471TriethylamineHCID 9590p-FluoronitrobenzeneHCID 46255812,4-Dimethylbenzene-1,3-diamine

Produkt 1

HCID 58794783HCID 58794783, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 679Dimethyl SulfoxideLösungsmittel

Reaktionsbedingungen

Temperatur
60 °C

Versuchsvorschrift

1.73 g of para-fluoronitrobenzene (2 eq.) were dissolved in 5 ml of DMSO. 1.2 equivalents of m-xylenediamine and 4 equivalents of triethylamine were added to the solution. The reaction mixture was heated at 60° C. for 20 hours. The mixture was then poured onto crushed ice and a precipitate formed. The latter was filtered, washed with water, and then dried.

Aufarbeitung

  1. additionThe mixture was then poured
  2. customonto crushed ice
  3. customa precipitate formed
  4. filtrationThe latter was filtered
  5. washwashed with water
  6. customdried

Quellen und Nachweise

ORD-Eintrag
ord-e6dc97c099be42f593855bc0cd045bfe
Quelldatensatz
uspto-grants-2008_09
Patentnummer
US07422609B2

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