HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Bromo-5-methoxybenzoic acid → 5-Methoxy-2-pyridin-3-ylbenzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Bromo-5-methoxybenzoic acid | HCID 89906 | — |
| Edukt | N-Methoxy-N-methylnicotinamide | HCID 10558996 | — |
| Edukt | Butyllithium | HCID 178418339 | — |
| Produkt | 5-Methoxy-2-pyridin-3-ylbenzoic acid | HCID 46315937 | — |
Reaktionsschritte
This compound is synthesized according to the method described in 3.2. by reacting 2-bromo-5-methoxybenzoic acid pretreated with n-butyllithium with N-methoxy-N-methylnicotinamide. After precipitation in aqueous phase at pH 4, followed by filtration and drying, a beige-coloured powder is obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07423030B2 |
| Quelldatensatz | uspto-grants-2008_09 |
| ORD ID | ord-3ea30621b6904a65840e6a85fe72c5cc |
| Quellennotiz | uspto-grants-2008_09 |