HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Bromo-3'-chloroacetophenone → (RS)-2-[2-(3-Chloro-phenyl)-2-oxo-ethoxycarbonylmethyl]-piperidine-1-carboxylic tert butyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Bromo-3'-chloroacetophenone | HCID 38738 | — |
| Edukt | 1-Boc-2-Piperidineacetic Acid | HCID 5058536 | — |
| Produkt | (RS)-2-[2-(3-Chloro-phenyl)-2-oxo-ethoxycarbonylmethyl]-piperidine-1-carboxylic tert butyl ester | HCID 86629011 | 81,4% |
Reaktionsschritte
The title compound (2.65 g) was prepared from (RS)-2-carboxymethyl-piperidine-1-carboxylic acid tert butyl ester (2.0 g) and 2-bromo-3′-chloroacetophenone (1.92 g) according to the method of description 36.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07423052B2 |
| Quelldatensatz | uspto-grants-2008_09 |
| ORD ID | ord-c95c2991bde54740a6af9825fb19498d |
| Quellennotiz | uspto-grants-2008_09 |