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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 31032Erstellt: 24. Oktober 2026

Ethanamine, 2,2,2-trifluoro- → (2,2,2-Trifluoro-ethyl)-carbamic acid (S)-1-[(S)-5-(2-benzyloxy-ethyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-ylcarbamoyl]-ethyl ester

https://huagongshe.com/de/reaction/31032

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthanamine, 2,2,2-trifluoro-HCID 9773—
EduktCarbonic acid (S)-1-[(S)-5-(2-benzyloxy-ethyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-ylcarbamoyl]-ethyl ester 4-nitro-phenyl esterHCID 58972494—
Produkt(2,2,2-Trifluoro-ethyl)-carbamic acid (S)-1-[(S)-5-(2-benzyloxy-ethyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-ylcarbamoyl]-ethyl esterHCID 58972461—

Reaktionsschritte

Using carbonic acid (S)-1-[(S)-5-(2-benzyloxy-ethyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-ylcarbamoyl]-ethyl ester 4-nitro-phenyl ester and 2,2,2-trifluoroethylamine, the title compound was prepared in the same manner as described for example 5c. Colorless, waxy solid (94%). MS: m/e=556(M+H+).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07425551B2
Quelldatensatzuspto-grants-2008_09
ORD IDord-3a187e9063d84744aac66dc088602c95
Quellennotizuspto-grants-2008_09