HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Imidazoline → 1-(4-Ethylphenyl)-2-imidazolylethan-1-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Imidazoline | HCID 68156 | — |
| Edukt | 2-Bromo-1-(4-ethylphenyl)ethan-1-one | HCID 12401951 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | 1-(4-Ethylphenyl)-2-imidazolylethan-1-one | HCID 22142578 | — |
Reaktionsschritte
1 mmol of 2-bromo-1-(4-ethylphenyl)ethan-1-one in acetonitrile was added drop wise to 5.5 mmol imidazoline in acetonitrile at room temperature for fourteen hours. The reaction mixture was concentrated in vacuo and diluted with water and ethyl acetate. The solution was extracted three times with ethyl acetate and dried over sodium sulfate to obtain 1-(4-ethylphenyl)-2-imidazolylethan-1-one.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07425557B2 |
| Quelldatensatz | uspto-grants-2008_09 |
| ORD ID | ord-24ee89c2f0684d92a2fe9090065cfceb |
| Quellennotiz | uspto-grants-2008_09 |