HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-(Chloromethyl)-3-phenyl-1,2,4-oxadiazole → HCID 22009808, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-(Chloromethyl)-3-phenyl-1,2,4-oxadiazole | HCID 966714 | — |
| Edukt | 1-[3-(4-Hydroxyphenyl)propyl]imidazole | HCID 22009818 | — |
| Produkt | HCID 22009808 | HCID 22009808 | 51% |
Reaktionsschritte
In substantially the same manner as in Working Example 72, 1-[3-(4-hydroxyphenyl)propyl]imidazole was reacted with 5-chloromethyl-3-phenyl-1,2,4-oxadiazole to obtain 5-[4-[3-(1-imidazolyl)propyl]phenoxymethyl]-3-phenyl-1,2,4-oxadiazole. The yield was 51%. Recrystallization from ethyl acetate-hexane gave colorless needles, mp 124-125° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06211215B1 |
| Quelldatensatz | uspto-grants-2001_04 |
| ORD ID | ord-e96274777f7c40f3ae3b13fbf018a3a9 |
| Quellennotiz | uspto-grants-2001_04 |