HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Leucine methyl ester hydrochloride → N-[N-(Phenylacetyl)-L-alaninyl]-L-leucine Methyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Leucine methyl ester hydrochloride | HCID 2723695 | — |
| Edukt | N-(Phenylacetyl)-L-alanine | HCID 7004640 | — |
| Produkt | N-[N-(Phenylacetyl)-L-alaninyl]-L-leucine Methyl Ester | HCID 9923756 | — |
Reaktionsschritte
Following General Procedure A and using N-(phenylacetyl)-L-alanine (from Example B1 above) and L-leucine methyl ester hydrochloride (Aldrich), the title compound was prepared as a solid (mp=102.5-105° C.). The reaction was monitored by tlc (Rf=0.25 in 50% EtOAc/hexanes).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06211235B1 |
| Quelldatensatz | uspto-grants-2001_04 |
| ORD ID | ord-7ff7abca63b649faafc14b1b9903e598 |
| Quellennotiz | uspto-grants-2001_04 |